CLOSED Version 2.0 Language English Run 1 RunSerial 2290 Instrument SDT Q600 V20.9 Build 20 Module DSC-TGA Standard InstSerial 0600-1010 Operator bnr File \\Hp16391794916\ta\Data\SDT\AAV\SUJITHA\MS-40@7.5C0 Sample MS-40@7.5C Size 1.39200 mg ProcName Ramp Method Ramp Comment ACRHEM, University of Hyderabad Xcomment Pan: Alumina Xcomment Gas1: Nitrogen 100.0 ml/min Xcomment Gas2: Nitrogen 0.0 ml/min Text Exotherm Up Kcell 1.00000 InstCalDate Weight: 2015-06-30 Time: 17:13:48 TempRange 50.07 to 1001.76 °C InstCalFile Weight: \\Hp16391794916\ta\Data\SDT\Calib\Baseline300615wo.001 \\Hp16391794916\ta\Data\SDT\Calib\Baseline300615ww.001 InstCalDate Heat Flow: 2015-07-08 Time: 13:05:45 TempRange 50.09 to 594.77 °C InstCalFile Heat Flow: \\Hp16391794916\ta\Data\SDT\Calib\DSCbaselinewo.001 \\Hp16391794916\ta\Data\SDT\Calib\DSCbaselinewsapphire.001 InstCalDate DTA Baseline: 2010-10-05 Time: 10:10:35 TempRange 500.16 to 1400.03 °C InstCalFile DTA Baseline: \\Mfg01-it-wxp\ta\Data\SDT\Oct\0600-1010\Beamwo.001 TempCal 2 pts 25.00 25.00,422.50 419.50 Controls Gas 1 Event OFF Sampling 0.5 sec/pt AutoAnalysis Off MacroFile Nsig 8 Sig1 Time (min) Sig2 Temperature (°C) Sig3 Weight (mg) Sig4 Heat Flow (mW) Sig5 Temperature Difference (°C) Sig6 Temperature Difference (µV) Sig7 Sample Purge Flow (mL/min) Sig8 Deriv. Weight (%/°C) Date 2016-02-25 Time 14:19:31 OrgMethod 1: Ramp 7.50 °C/min to 200.00 °C OrgFile C:\TA\Data\SDT\AAV\SUJITHA\MS-40@7.5C0 .003200000 25.48445 1.392345 -11.60010 -0.1076966 -0.6405474 100.0416 0.04297302 .004333333 25.49187 1.392066 -11.59999 -0.1076798 -0.6404534 99.94884 0.04297048 0.01266666 25.48804 1.392042 -11.60029 -0.1077208 -0.6407026 100.0132 0.04297180 0.02100000 25.48268 1.391950 -11.60102 -0.1078206 -0.6413009 100.0072 0.04297363 0.02933333 25.48425 1.391777 -11.60159 -0.1078986 -0.6417687 99.99344 0.04297309 0.03766667 25.48658 1.391746 -11.60241 -0.1080109 -0.6424412 99.97290 0.04297230 0.04600000 25.48942 1.391620 -11.60340 -0.1081474 -0.6432584 100.0072 0.04297133 0.05433334 25.48470 1.391469 -11.60458 -0.1083097 -0.6442288 100.0191 0.04297294 0.06266666 25.48785 1.391444 -11.60606 -0.1085136 -0.6454459 99.96961 0.04297186 0.07100000 25.49070 1.391295 -11.60773 -0.1087425 -0.6468130 100.0327 0.04297088 0.07933334 25.49246 1.391254 -11.60936 -0.1089670 -0.6481528 99.96999 0.04297028 0.08766666 25.48583 1.391483 -11.61134 -0.1092412 -0.6497834 100.0515 0.04297254 0.09600000 25.48799 1.391381 -11.61307 -0.1094794 -0.6512000 99.96126 0.04297180 0.1043333 25.48370 1.391455 -11.61431 -0.1096504 -0.6522164 99.99478 0.04297328 0.1126666 25.48615 1.391554 -11.61571 -0.1098438 -0.6533678 100.0240 0.04297244 0.1210000 25.48534 1.391512 -11.61697 -0.1100177 -0.6544015 99.99269 0.04297272 0.1293333 25.48562 1.391599 -11.61801 -0.1101612 -0.6552544 99.95676 0.04297262 0.1376667 25.48898 1.391631 -11.61913 -0.1103163 -0.6561774 100.0430 0.04297148 0.1460000 25.49070 1.391604 -11.62017 -0.1104597 -0.6570316 99.96775 0.04297089 0.1543334 25.49129 1.391664 -11.62151 -0.1106442 -0.6581298 100.0030 0.04297068 0.1626666 25.49265 1.391658 -11.62249 -0.1107796 -0.6589350 100.0377 0.04297022 0.1710000 25.49886 1.391654 -11.62328 -0.1108885 -0.6595847 99.95816 0.04296808 0.1793333 25.50101 1.391763 -11.62362 -0.1109353 -0.6598660 100.0188 0.04296734 0.1876666 25.50870 1.391675 -11.62442 -0.1110449 -0.6605235 99.99789 0.04296470 0.1960000 25.51536 1.391774 -11.62499 -0.1111224 -0.6609921 99.98644 0.04296240 0.2043333 25.51417 1.391752 -11.62539 -0.1111765 -0.6613216 99.99824 0.04296280 0.2126666 25.51967 1.391750 -11.62576 -0.1112266 -0.6616284 100.0147 0.04296090 0.2210000 25.52312 1.391798 -11.62567 -0.1112120 -0.6615501 99.96821 0.04295971 0.2293333 25.52140 1.391760 -11.62502 -0.1111216 -0.6610204 100.0433 0.04296031 0.2376666 25.52840 1.391804 -11.62401 -0.1109802 -0.6601889 99.95566 0.04295788 0.2460000 25.52825 1.391815 -11.62317 -0.1108631 -0.6595020 100.0133 0.04295793 0.2543334 25.53377 1.391786 -11.62218 -0.1107261 -0.6586958 100.0838 0.04295601 0.2626667 25.54666 1.391787 -11.62089 -0.1105464 -0.6576384 99.98908 0.04295152 0.2710000 25.54826 1.391773 -11.61861 -0.1102295 -0.6557641 99.99293 0.04258537 0.2793333 25.55066 1.391697 -11.61625 -0.1099028 -0.6538299 99.94331 0.04258404 0.2876667 25.55786 1.391756 -11.61386 -0.1095718 -0.6518708 100.0493 0.04258008 0.2960000 25.56194 1.391689 -11.61112 -0.1091924 -0.6496248 100.0028 0.04257783 0.3043333 25.57080 1.391702 -11.60822 -0.1087905 -0.6472458 99.99605 0.04257291 0.3126666 25.57542 1.391684 -11.60496 -0.1083384 -0.6445693 99.97165 0.04257034 0.3210000 25.58756 1.391609 -11.60096 -0.1077847 -0.6412898 100.0112 0.04256357 0.3293334 25.59631 1.391627 -11.59666 -0.1071892 -0.6377631 100.0205 0.04255867 0.3376666 25.59785 1.391580 -11.59193 -0.1065344 -0.6338840 99.96031 0.04255780 0.3460000 25.61435 1.391588 -11.58742 -0.1059089 -0.6301787 100.0283 0.04254850 0.3543334 25.62683 1.391614 -11.58276 -0.1052644 -0.6263620 99.94980 0.04216671 0.3626666 25.63840 1.391586 -11.57773 -0.1045675 -0.6222362 100.0146 0.04216376 0.3710000 25.64801 1.391578 -11.57199 -0.1037721 -0.6175250 100.0031 0.04216130 0.3793334 25.66768 1.391594 -11.56611 -0.1029571 -0.6126992 99.99070 0.04215626 0.3876666 25.67777 1.391534 -11.55954 -0.1020474 -0.6073120 100.0239 0.04215366 0.3960000 25.69092 1.391583 -11.55266 -0.1010955 -0.6016734 99.99000 0.04215025 0.4043333 25.70719 1.391540 -11.54562 -0.1001196 -0.5958930 99.97954 0.04178402 0.4126667 25.71414 1.391503 -11.53810 -.09907876 -0.5897259 99.97244 0.04178404 0.4210000 25.72752 1.391489 -11.53021 -.09798705 -0.5832571 100.0099 0.04178409 0.4293333 25.73834 1.391408 -11.52155 -.09678849 -0.5761518 100.0634 0.04178412 0.4376666 25.75590 1.391406 -11.51263 -.09555411 -0.5688332 99.96299 0.04178420 0.4460000 25.76684 1.391372 -11.50334 -.09426981 -0.5612160 100.0256 0.04178425 0.4543334 25.78228 1.391330 -11.49406 -.09298564 -0.5536007 99.98200 0.04144222 0.4626666 25.79760 1.391323 -11.48428 -.09163272 -0.5455742 100.0101 0.04143508 0.4710000 25.81728 1.391288 -11.47390 -.09019775 -0.5370594 99.98150 0.04142580 0.4793334 25.83818 1.391226 -11.46341 -.08874736 -0.5284537 100.0398 0.04141590 0.4876666 25.85482 1.391206 -11.45243 -.08723028 -0.5194503 99.96629 0.04106790 0.4960000 25.87534 1.391184 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