CLOSED Version 2.0 Language English Run 1 RunSerial 2289 Instrument SDT Q600 V20.9 Build 20 Module DSC-TGA Standard InstSerial 0600-1010 Operator bnr File \\Hp16391794916\ta\Data\SDT\AAV\SUJITHA\MS-40@5C.001 Sample MS-40@5C Size 1.16200 mg ProcName Ramp Method Ramp Comment ACRHEM, University of Hyderabad Xcomment Pan: Alumina Xcomment Gas1: Nitrogen 100.0 ml/min Xcomment Gas2: Nitrogen 0.0 ml/min Text Exotherm Up Kcell 1.00000 InstCalDate Weight: 2015-06-30 Time: 17:13:48 TempRange 50.07 to 1001.76 °C InstCalFile Weight: \\Hp16391794916\ta\Data\SDT\Calib\Baseline300615wo.001 \\Hp16391794916\ta\Data\SDT\Calib\Baseline300615ww.001 InstCalDate Heat Flow: 2015-07-08 Time: 13:05:45 TempRange 50.09 to 594.77 °C InstCalFile Heat Flow: \\Hp16391794916\ta\Data\SDT\Calib\DSCbaselinewo.001 \\Hp16391794916\ta\Data\SDT\Calib\DSCbaselinewsapphire.001 InstCalDate DTA Baseline: 2010-10-05 Time: 10:10:35 TempRange 500.16 to 1400.03 °C InstCalFile DTA Baseline: \\Mfg01-it-wxp\ta\Data\SDT\Oct\0600-1010\Beamwo.001 TempCal 2 pts 25.00 25.00,422.50 419.50 Controls Gas 1 Event OFF Sampling 0.5 sec/pt AutoAnalysis Off MacroFile Nsig 8 Sig1 Time (min) Sig2 Temperature (°C) Sig3 Weight (mg) Sig4 Heat Flow (mW) Sig5 Temperature Difference (°C) Sig6 Temperature Difference (µV) Sig7 Sample Purge Flow (mL/min) Sig8 Deriv. Weight (%/°C) Date 2016-02-25 Time 11:27:48 OrgMethod 1: Ramp 5.00 °C/min to 200.00 °C OrgFile C:\TA\Data\SDT\AAV\SUJITHA\MS-40@5C.001 6.66667E-4 27.84440 1.161793 -12.34308 -0.2084314 -1.251586 99.98781 0.05757685 .004333333 27.84985 1.161677 -12.34739 -0.2090354 -1.255115 100.0090 0.05757370 0.01266666 27.84422 1.161605 -12.34768 -0.2090746 -1.255356 99.97079 0.05757695 0.02100000 27.84058 1.161556 -12.34801 -0.2091195 -1.255628 100.0192 0.05757905 0.02933333 27.84548 1.161393 -12.34874 -0.2092184 -1.256225 100.0020 0.05757622 0.03766667 27.84026 1.161361 -12.34968 -0.2093464 -1.256997 100.0256 0.05757922 0.04600000 27.83885 1.161244 -12.35087 -0.2095091 -1.257976 99.94981 0.05758004 0.05433334 27.84230 1.161094 -12.35220 -0.2096903 -1.259067 100.0414 0.05757806 0.06266666 27.83935 1.161046 -12.35369 -0.2098942 -1.260293 99.96912 0.05757974 0.07100000 27.83460 1.160918 -12.35532 -0.2101164 -1.261628 100.0138 0.05758247 0.07933334 27.83408 1.160842 -12.35698 -0.2103436 -1.262990 99.96828 0.05758277 0.08766666 27.83190 1.160969 -12.35851 -0.2105534 -1.264245 100.0245 0.05758402 0.09600000 27.82570 1.160917 -12.36000 -0.2107580 -1.265464 99.99672 0.05758756 0.1043333 27.83114 1.160921 -12.36178 -0.2110034 -1.266930 100.0026 0.05758445 0.1126666 27.82973 1.160996 -12.36321 -0.2111996 -1.268102 100.0364 0.05758526 0.1210000 27.82726 1.160902 -12.36446 -0.2113717 -1.269127 99.96080 0.05758666 0.1293333 27.82794 1.160984 -12.36535 -0.2114944 -1.269859 100.0217 0.05758629 0.1376667 27.82850 1.160996 -12.36623 -0.2116156 -1.270579 99.98187 0.05758596 0.1460000 27.82936 1.160954 -12.36727 -0.2117584 -1.271430 99.98472 0.05758547 0.1543334 27.82998 1.161004 -12.36801 -0.2118601 -1.272038 99.99819 0.05758511 0.1626666 27.82822 1.160946 -12.36888 -0.2119798 -1.272755 100.0080 0.05758612 0.1710000 27.82927 1.160943 -12.36982 -0.2121086 -1.273526 99.99488 0.05758552 0.1793333 27.82374 1.160981 -12.37081 -0.2122439 -1.274336 100.0415 0.05758868 0.1876666 27.81744 1.160926 -12.37102 -0.2122731 -1.274509 99.95562 0.05759228 0.1960000 27.82547 1.160957 -12.37139 -0.2123252 -1.274816 100.0107 0.05758770 0.2043333 27.82748 1.160927 -12.37192 -0.2123982 -1.275253 100.0124 0.05758655 0.2126666 27.82760 1.160863 -12.37238 -0.2124600 -1.275625 99.98292 0.05758648 0.2210000 27.83055 1.160917 -12.37289 -0.2125296 -1.276044 100.0330 0.05758479 0.2293333 27.83264 1.160868 -12.37292 -0.2125335 -1.276068 99.96080 0.05758359 0.2376666 27.83625 1.160874 -12.37293 -0.2125350 -1.276079 100.0256 0.05758152 0.2460000 27.83113 1.160898 -12.37224 -0.2124402 -1.275513 99.99012 0.05758445 0.2543334 27.82920 1.160825 -12.37159 -0.2123516 -1.274982 100.0010 0.05758557 0.2626667 27.83135 1.160830 -12.37078 -0.2122402 -1.274316 99.99205 0.05758434 0.2710000 27.83360 1.160794 -12.36992 -0.2121216 -1.273608 99.98094 0.05758305 0.2793333 27.83958 1.160760 -12.36854 -0.2119324 -1.272480 100.0048 0.05757961 0.2876667 27.84271 1.160802 -12.36674 -0.2116838 -1.270996 100.0498 0.05757782 0.2960000 27.84169 1.160774 -12.36488 -0.2114287 -1.269470 99.98281 0.05757840 0.3043333 27.84910 1.160754 -12.36256 -0.2111110 -1.267572 99.97664 0.05757414 0.3126666 27.85756 1.160740 -12.35990 -0.2107455 -1.265388 100.0207 0.05708460 0.3210000 27.86302 1.160650 -12.35688 -0.2103308 -1.262912 100.0195 0.05708228 0.3293334 27.86461 1.160667 -12.35385 -0.2099140 -1.260425 100.0181 0.05708160 0.3376666 27.85630 1.160654 -12.35042 -0.2094425 -1.257608 99.97504 0.05708513 0.3460000 27.86248 1.160654 -12.34694 -0.2089642 -1.254750 99.99792 0.05708251 0.3543334 27.86844 1.160679 -12.34320 -0.2084503 -1.251682 99.96769 0.05707998 0.3626666 27.87468 1.160621 -12.33924 -0.2079069 -1.248436 100.0446 0.05707731 0.3710000 27.87885 1.160616 -12.33466 -0.2072769 -1.244670 99.97588 0.05707554 0.3793334 27.88482 1.160588 -12.32991 -0.2066246 -1.240775 100.0355 0.05707298 0.3876666 27.88993 1.160528 -12.32481 -0.2059243 -1.236589 99.92726 0.05707079 0.3960000 27.89548 1.160534 -12.31951 -0.2051968 -1.232240 100.0421 0.05706840 0.4043333 27.90850 1.160531 -12.31433 -0.2044863 -1.227993 100.0416 0.05658738 0.4126667 27.91306 1.160509 -12.30876 -0.2037205 -1.223417 99.94892 0.05658676 0.4210000 27.91644 1.160488 -12.30252 -0.2028641 -1.218301 100.0212 0.05658630 0.4293333 27.93478 1.160409 -12.29538 -0.2018828 -1.212440 99.98856 0.05658382 0.4376666 27.94260 1.160393 -12.28800 -0.2008692 -1.206388 100.0010 0.05658278 0.4460000 27.94772 1.160399 -12.28031 -0.1998121 -1.200074 100.0282 0.05658208 0.4543334 27.95246 1.160352 -12.27274 -0.1987719 -1.193861 99.97400 0.05658144 0.4626666 27.96516 1.160336 -12.26437 -0.1976232 -1.186999 99.99387 0.05657974 0.4710000 27.96862 1.160297 -12.25579 -0.1964446 -1.179957 99.99981 0.05612598 0.4793334 27.98725 1.160254 -12.24691 -0.1952244 -1.172667 100.0189 0.05612200 0.4876666 27.99194 1.160230 -12.23730 -0.1939056 -1.164786 99.99791 0.05612100 0.4960000 28.00810 1.160175 -12.22747 -0.1925558 -1.156719 100.0255 0.05611753 0.5043333 28.02010 1.160178 -12.21709 -0.1911296 -1.148198 99.99272 0.05567991 0.5126667 28.02920 1.160163 -12.20622 -0.1896378 -1.139280 99.99586 0.05567742 0.5210000 28.04325 1.160111 -12.19519 -0.1881242 -1.130231 99.97164 0.05567356 0.5293334 28.05545 1.160080 -12.18363 -0.1865380 -1.120747 99.98300 0.05567021 0.5376668 28.06672 1.160018 -12.17136 -0.1848542 -1.110680 100.0250 0.05566709 0.5460000 28.08373 1.159978 -12.15903 -0.1831619 -1.100562 100.0278 0.05523730 0.5543332 28.09438 1.159969 -12.14616 -0.1813948 -1.089997 99.97265 0.05523174 0.5626668 28.10654 1.159925 -12.13269 -0.1795473 -1.078948 100.0274 0.05522537 0.5710000 28.12699 1.159919 -12.11899 -0.1776676 -1.067708 99.99281 0.05479306 0.5793332 28.14416 1.159897 -12.10505 -0.1757545 -1.056267 99.98228 0.05478692 0.5876668 28.15402 1.159858 -12.09078 -0.1737962 -1.044553 99.98868 0.05478338 0.5960000 28.17520 1.159828 -12.07621 -0.1717977 -1.032598 99.98091 0.05436260 0.6043334 28.19025 1.159790 -12.06097 -0.1697074 -1.020094 100.0102 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-11.82611 -0.1375241 -0.8273820 99.93618 0.05266915 0.7210000 28.46123 1.159456 -11.80531 -0.1346771 -0.8103188 100.0222 0.05227002 0.7293334 28.48418 1.159441 -11.78462 -0.1318452 -0.7933450 99.97789 0.05225872 0.7376666 28.50560 1.159419 -11.76316 -0.1289085 -0.7757368 100.0275 0.05224810 0.7460000 28.53004 1.159407 -11.74125 -0.1259102 -0.7577579 99.97658 0.05184500 0.7543334 28.56004 1.159390 -11.71887 -0.1228472 -0.7393882 100.0127 0.05183458 0.7626666 28.58186 1.159364 -11.69651 -0.1197885 -0.7210412 99.98425 0.05143850 0.7710000 28.60915 1.159334 -11.67350 -0.1166425 -0.7021662 100.0156 0.05143347 0.7793334 28.63432 1.159289 -11.64969 -0.1133863 -0.6826259 99.98046 0.05105276 0.7876668 28.65850 1.159234 -11.62535 -0.1100585 -0.6626522 100.0169 0.05105547 0.7960000 28.68996 1.159208 -11.60056 -0.1066697 -0.6423093 99.97914 0.05070480 0.8043334 28.72103 1.159185 -11.57551 -0.1032473 -0.6217628 100.0195 0.05069826 0.8126668 28.75331 1.159172 -11.54978 -.09973145 -0.6006523 100.0127 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0.1316214 0.7985835 99.96266 0.04024848 1.246000 30.72537 1.158296 -9.805650 0.1368389 0.8303872 100.0337 0.04001555 1.254334 30.77726 1.158282 -9.766359 0.1421255 0.8626234 99.94601 0.03977902 1.262667 30.82476 1.158277 -9.726986 0.1474209 0.8949269 100.0480 0.03954834 1.271000 30.87727 1.158257 -9.687430 0.1527388 0.9273798 99.96795 0.03954403 1.279334 30.92232 1.158256 -9.647859 0.1580562 0.9598446 99.99494 0.03932418 1.287666 30.97058 1.158245 -9.607981 0.1634135 0.9925629 100.0536 0.03911035 1.296000 31.01846 1.158231 -9.567900 0.1687963 1.025448 99.91222 0.03889870 1.304334 31.07492 1.158201 -9.527811 0.1741772 1.058338 100.0402 0.03869233 1.312666 31.11577 1.158203 -9.487656 0.1795650 1.091282 99.95699 0.03849094 1.321000 31.16678 1.158190 -9.447382 0.1849666 1.124323 100.0040 0.03829918 1.329334 31.21308 1.158150 -9.406844 0.1904022 1.157584 99.98951 0.03829477 1.337666 31.26431 1.158127 -9.366088 0.1958649 1.191020 100.0118 0.03810163 1.346000 31.31047 1.158115 -9.325374 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