Dataset for " Phosphorylthioformic Acid Hydrazides: A New Polyheteroatom Reagents for the Synthesis of Phosphorus(V)-Substituted Aza-heterocycles"
The raw 1H, 13C, 31P NMR FID files, copies of IR and HRMS spectra for representative compounds are available.
Steps to reproduce
NMR spectra were acquired at room temperature; the chemical shifts δ were measured in ppm relative to the solvent (1Н: CDCl3, δ = 7.27 ppm, DMSO-d6, δ = 2.50 ppm; 13C: CDCl3, δ = 77.00 ppm, DMSO-d6, δ = 39.50 ppm). Splitting patterns are designated as s, singlet; d, doublet; t, triplet; q, quartet; m, multiplet; dd, double doublet;. The coupling constants (J) are in Hertz. High-resolution and accurate mass spectra were obtained on BrukermicrOTOF-QTM ESI-TOF (Electrospray Ionization/Time of Flight) and Thermo Scientific* LTQ Orbitrap mass spectrometers.
Russian Science Foundation