Dataset for " Phosphorylthioformic Acid Hydrazides: A New Polyheteroatom Reagents for the Synthesis of Phosphorus(V)-Substituted Aza-heterocycles"
Published: 17 October 2023| Version 2 | DOI: 10.17632/2537f6mpxh.2
Contributor:
Yulia VolkovaDescription
The raw 1H, 13C, 31P NMR FID files, copies of IR and HRMS spectra for representative compounds are available.
Files
Steps to reproduce
NMR spectra were acquired at room temperature; the chemical shifts δ were measured in ppm relative to the solvent (1Н: CDCl3, δ = 7.27 ppm, DMSO-d6, δ = 2.50 ppm; 13C: CDCl3, δ = 77.00 ppm, DMSO-d6, δ = 39.50 ppm). Splitting patterns are designated as s, singlet; d, doublet; t, triplet; q, quartet; m, multiplet; dd, double doublet;. The coupling constants (J) are in Hertz. High-resolution and accurate mass spectra were obtained on BrukermicrOTOF-QTM ESI-TOF (Electrospray Ionization/Time of Flight) and Thermo Scientific* LTQ Orbitrap mass spectrometers.
Institutions
Institut organiceskoj himii imeni N D Zelinskogo
Categories
Nuclear Magnetic Resonance Spectroscopy, 31P NMR Spectroscopy, 13C NMR Spectroscopy
Funding
Russian Science Foundation
22-13-00161