Dataset for " Phosphorylthioformic Acid Hydrazides: A New Polyheteroatom Reagents for the Synthesis of Phosphorus(V)-Substituted Aza-heterocycles"

Published: 17 October 2023| Version 2 | DOI: 10.17632/2537f6mpxh.2
Contributor:
Yulia Volkova

Description

The raw 1H, 13C, 31P NMR FID files, copies of IR and HRMS spectra for representative compounds are available.

Files

Steps to reproduce

NMR spectra were acquired at room temperature; the chemical shifts δ were measured in ppm relative to the solvent (1Н: CDCl3, δ = 7.27 ppm, DMSO-d6, δ = 2.50 ppm; 13C: CDCl3, δ = 77.00 ppm, DMSO-d6, δ = 39.50 ppm). Splitting patterns are designated as s, singlet; d, doublet; t, triplet; q, quartet; m, multiplet; dd, double doublet;. The coupling constants (J) are in Hertz. High-resolution and accurate mass spectra were obtained on BrukermicrOTOF-QTM ESI-TOF (Electrospray Ionization/Time of Flight) and Thermo Scientific* LTQ Orbitrap mass spectrometers.

Institutions

Institut organiceskoj himii imeni N D Zelinskogo

Categories

Nuclear Magnetic Resonance Spectroscopy, 31P NMR Spectroscopy, 13C NMR Spectroscopy

Funding

Russian Science Foundation

22-13-00161

Licence