Hydrolysis data for bis(4-cyanophenyl) phenyl phosphate
Published: 24 October 2019| Version 1 | DOI: 10.17632/3fmv6p3smk.1
Contributors:
Vladimir Terekhov, Vladislav Aleshkevich, Ekaterina Afanaseva, Sergei Nechausov, Aleksandr Babkin, Boris Bulgakov, Aleksei Kepman, Viktor AvdeevDescription
This dataset obtained from hydrolysis process of bis(4-cyanophenyl) phenyl phosphate (CPP). The dataset contains raw NMR-spectroscopy data of CPP and products of hydrolysis (can be open with e.g. ACDLabs Spectrus processor) as 1H, 13C, 31P NMR free induction decays (FID), raw HPLC chromatograms including initial chromatograms of CPP, 4-cyanophenol and phenol, and chromatograms obtained during hydrolysis study (.pdf). Hydrolysis was carried out under pH 4, 7, 10 and at temperatures of 25, 35, 50, 60 and 80°C. Two series of aliquots were selected from the reaction mixture in certain time periods to obtain the average values of the peak areas in the chromatograms.
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Categories
Chemistry, Chemical Compounds in Materials Science