Data for the synthesis, characterization, and use of xerogels as adsorbents for the removal of fluoride and bromide in aqueous phase

Published: 31 March 2022| Version 2 | DOI: 10.17632/gvjd33sw57.2
Contributors:
Nahum Andres Medellin Castillo, Elizabeth Diane Isaacs-Páez, Liliana Giraldo-Gutierrez, Juan Carlos Moreno-Pirajan, Itzia Rodriguez-Mendez, Simon Yobanny Reyes-Lopez, Jaime Reyes-Henandez, Sonia Judith Segovia-Sandoval

Description

Xerogels were synthesized using the methodology proposed by Muehlemann et al. The xerogels M/R=0.5 were carbonized in a horizontal tubular furnace Carbolite model 12/65/550 under a N2 flow at 400, 450, and 550 °C for 2 h. The equilibrium adsorption experiments were carried out in a batch adsorber using 0.02 g of carbonized xerogel, 50 mL of fluoride, or bromide solution with different initial concentrations ranging from 10 to 100 mg L-1. The experiments were carried out at constant pH. The mass of fluoride or bromide adsorbed per gram of adsorbent (q), was obtained using a mass balance equation. The adsorption equilibrium data were fitted by Langmuir, Freundlich and Prausnitz-Radke isotherm models.The bromide and fluoride concentration in aqueous solution was measured by a potentiometric method with a bromide or fluoride ion-selective electrode.

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Institutions

  • Instituto Potosino de Investigacion Cientifica y Tecnologica
  • Universidad Autonoma de San Luis Potosi
  • Universidad Autonoma de Ciudad Juarez
  • Universidad de los Andes

Categories

Water Treatment, Adsorption, Fluoride, Xerogels, Bromate

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