Data on peculiarities of microstructure of diffusion zone and reaction zone in Al-Co system

Published: 21 Feb 2020 | Version 2 | DOI: 10.17632/n7pkjjb25r.2
Contributor(s):
  • Gulzira Ibrayeva,
    Materials Science
    1Institute of Metallurgy and Ore Beneficiation", Satbayev University
  • Bulat Sukurov
    Bulat Sukurov
    Institute of Metallurgy and Ore Beneficiation, Satbayev University
    Conceptualization, Data curation, Funding acquisition, Investigation, Methodology, Software, Supervision, Validation, Writing - review & editing.

Description of this data

Raw data

  1. Backscattered electron image of intermetallic multilayer zone in Al-Co system.
    Instrument: 8230, 25 kV
  2. Energy dispersive linear X-ray analysis of diffusion and reaction zone of Al-Co system.
    Instrument: 8230, 25 kV, 5 nA (on picture is not registered), DT: 18.0%, Count Rate: 9,973.00 CPS
  3. Wavelength dispersive linear X-ray analysis of diffusion and reaction zone of Al-Co system. (in the same area).
    Instrument: 8230, 20 kV, 9.78 nA Dwell Time: 500.00 ms
    Al on TAP: Ka 1 Line
    Co on LiF: Ka 1 Line

Experiment data files

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Steps to reproduce

Samples of Al-Co systems were prepared by means of the diffusion couple method (contact smelting). This method used the mode “Solid metal Co – liquid aluminum” at temperature 1350ºС for 1 hour with subsequuent cooling in furnace. Aluminum A99 Grade, cobalt K0 Grade (Terms are taken in Russian).
For sample preparations in the longitudinal and cross sections STRUERS equipment (Secotom-50 and Tegramin-25) was used. Studies of scanning electron microscopy (SEM) and electron probe microanalysis (EPMA) were implemented using the microanalyzer JXA-8230 (JEOL).
EDS and WDS analyses were performed at cross-sectional observation.

Latest version

  • Version 2

    2020-02-21

    Published: 2020-02-21

    DOI: 10.17632/n7pkjjb25r.2

    Cite this dataset

    Ibrayeva, Gulzira; Sukurov, Bulat (2020), “Data on peculiarities of microstructure of diffusion zone and reaction zone in Al-Co system”, Mendeley Data, v2 http://dx.doi.org/10.17632/n7pkjjb25r.2

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Categories

Materials Science, Aluminide

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