SCALPEL 3D

Published: 22 December 2018| Version 1 | DOI: 10.17632/tbhmz5396m.1
Contributor:
Guilherme Dal Poggetto

Description

i) TopSpin files a) AU program: setscalpelpars b) Pulse sequence for BRUKER: SCALPEL_it2 c) Pulse sequence for BRUKER: SCALPEL_idiff d) Pulse sequence for BRUKER: gdp_2dsel_it2_dipsi e) Pulse sequence for BRUKER: gdp_2dsel_idiff_dipsi ii) SCALPEL data (BRUKER format) a)Glucose, glucose-6-phosphate and maltose, in D2O (FOLDER Glucose_gluc6P_maltose) 1 - 1H 2 - 2D 1H Oneshot45, with water pre-saturation 3 - 2D 1H iDESTO, with water pre-saturation 4 - 1H selective TOCSY 5 - 3D SCALPEL (using TOCSY-t1 and diffusion) b)Lactose and melibiose, in D2O (FOLDER Lactose_melibiose) 1 - 1H 2 - 2D 1H iREST2, with water pre-saturation 3 - 2D SCALPEL (first increment of TOCSY-t1 and relaxation decay), with water pre-saturation 4 - 3D SCALPEL (using TOCSY-t1 and relaxation), with water pre-saturation c)Mackeson Stout, with 20% added D2O (FOLDER Stout_20%D2O) 1 - 1H 2 - 2D 1H Oneshot45, with water pre-saturation 3 - 2D 1H iDESTO with, water pre-saturation 4 - 1H, with water pre-saturation 5 - {1H}13C 6 - 2D EA-HSQC 7 - 2D EA-HSQC-TOCSY 8 - 3D SCALPEL (using TOCSY-t1 and diffusion) 9 - 3D SCALPEL (using TOCSY-t1 and relaxation) 10 - 1H selective TOCSY 11 - 3D SCALPEL (using TOCSY-t1 and diffusion), with water pre-saturation

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Institutions

The University of Manchester

Categories

Analytical Chemistry, Carbohydrates, NMR Pulse

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