Microporous and Mesoporous Materials

The folder contains images and EDX spectra of nano ZSM-5 crystals. The readme-file explains how data is structured and was acquired.

Magnetic propoerties of the Composite materials

the data of N2 adsorption, XRD, 27Al/31P MAS NMR, NH3-TPD and Py/Coll-FTIR

Raw data and Figures

The dataset contains the data supporting the publication in Microporous and Mesoporous Materials, Volume 378 (2024), Article 113234. It includes XRD patterns, N2 physisorption isotherms, microscopy images, IR, UV-Vis and NMR spectra of the studied materials as well as their catalytic behaviour in transfromation of sucrose to HMF in terms of conversion, selectivity and yield.

Dataset that contains different data on electrochemical and x-ray diffraction experiments of the synthesis and structure investigations of hybrid materials made out of conductive polymers and porous silicon. The mesoporous silicon epilayers are filled electrochemically with the polymers polypyrrole and poly-3,4-ethylendioxythiophen. Polyaniline could only be deposited on top of the porous silicon and not inside the mesopores. If applicable, the galvanostatic raw datasets have to normalized by the epilayer surface area of 7.89cm². The x-ray diffraction data contains both powder diffraction data sets (counts vs. 2-theta) and 2D detector images (P08 DESY synchrotron, 25 keV) of the monomer 2,5-Dibromo-3,4-ethylenedioxythiophene and the polymer poly-3,4-ethylendioxythiophen after solid state polymerization at 60°C. The samples investigated at the synchrotron (2D datasets) are hybrid materials in which the mesoporous pore space of the silicon is filled via spontaneous imbibition of the DBEDOT and subsequently polymerized to PEDOT. Each 2D image is taken at a different z position in order to mitigate beam damage.

Supporting Information for the paper "Zeolite-catalyzed one-pot sucrose-to-HMF transformation: Ge outperforms Sn, Zr, and Al sites"

Replication data for the figures in the manuscript

All primary data files of measurements and processed data of the journal article "Comparative study of lattice parameter and pore size of ordered mesoporous silica materials using physisorption, SAXS measurements and transmission electron microscopy", are deposited. File types which are not easily readable have been converted to other formats, i.e. TIF and TXT, and have been deposited additionally. PDH files may be opened with the same applications as TXT files.

The dataset contains the following data: nitrogen physisorption measurements, small-angle X-ray scattering curves, transmission electron micrographs. The data is named according to the sample name. A short description of the samples is given in the following:

OMS_TLCT: Ordered mesoporous silica material synthesized via true liquid crystal templating with hexadecylethyldimethylammonium chloride as surfactant

MCM-41: Ordered mesoporous silica material synthesized via a cooperative self-assembly process with hexadecyltrimethylammonium chloride as surfactant

SBA-15: Ordered mesoporous silica material synthesized via a cooperative self-assembly process with the poloxamer P123 as surfactant

SBA-15_sa: Ordered mesoporous silica material synthesized via a cooperative self-assembly process with the poloxamer P123 as surfactant and n-decane as swelling agent

Raw data sets from low angle powder XRD, N2 porosimetry, STEM and SEM