Data on peculiarities of microstructure of diffusion zone and reaction zone in Al-Co system
Raw data 1. Backscattered electron image of intermetallic multilayer zone in Al-Co system. Instrument: 8230, 25 kV 2. Energy dispersive linear X-ray analysis of diffusion and reaction zone of Al-Co system. Instrument: 8230, 25 kV, 5 nA (on picture is not registered), DT: 18.0%, Count Rate: 9,973.00 CPS 3. Wavelength dispersive linear X-ray analysis of diffusion and reaction zone of Al-Co system. (in the same area). Instrument: 8230, 20 kV, 9.78 nA Dwell Time: 500.00 ms Al on TAP: Ka 1 Line Co on LiF: Ka 1 Line
Steps to reproduce
Samples of Al-Co systems were prepared by means of the diffusion couple method (contact smelting). This method used the mode “Solid metal Co – liquid aluminum” at temperature 1350ºС for 1 hour with subsequuent cooling in furnace. Aluminum A99 Grade, cobalt K0 Grade (Terms are taken in Russian). For sample preparations in the longitudinal and cross sections STRUERS equipment (Secotom-50 and Tegramin-25) was used. Studies of scanning electron microscopy (SEM) and electron probe microanalysis (EPMA) were implemented using the microanalyzer JXA-8230 (JEOL). EDS and WDS analyses were performed at cross-sectional observation.