A mild, efficient and rapid protocol the removal of alcoholic TBDMS ethers using PVP-1 as catalyst in methanol, the procedure of deprotection of various TBDMS ethers were found to be very convenient, easy work-up, high yielding. All the compounds are unambiguously characterized by spectroscopic data. The experimental procedures were fully reproducible.
Contributors:López-González, Ricardo, Gnecco, Dino, Juárez, Jorge R., Orea, María L., Gómez-Calvario, Victor, Bernès, Sylvain, Aparicio, David M., Terán, Joel L.
Related Article: Ricardo López-González, Dino Gnecco, Jorge R. Juárez, María L. Orea, Victor Gómez-Calvario, Sylvain Bernès, David M. Aparicio, Joel L. Terán|2020|Tetrahedron Lett.|61|151697|doi:10.1016/j.tetlet.2020.151697